Cure Kinetics of Advanced Epoxy Molding Compound Using Dynamic Heating Scan
공공데이터포털
The data are associated with figures in R. Tao, S. P. Phansalkar, A. M. Forster, B. Han, Investigation of Cure Kinetics of Advanced Epoxy Molding Compound Using Dynamic Heating Scan: An Overlooked Second Reaction, 2023 IEEE 73rd Electronic Components and Technology Conference (ECTC), Orlando, Florida, May 30 - June 2, 2023. https://doi.org/10.1109/ECTC51909.2023.00225
Cure Kinetics of Advanced Epoxy Molding Compound Using Dynamic Heating Scan
공공데이터포털
The data are associated with figures in R. Tao, S. P. Phansalkar, A. M. Forster, B. Han, Investigation of Cure Kinetics of Advanced Epoxy Molding Compound Using Dynamic Heating Scan: An Overlooked Second Reaction, 2023 IEEE 73rd Electronic Components and Technology Conference (ECTC), Orlando, Florida, May 30 - June 2, 2023. https://doi.org/10.1109/ECTC51909.2023.00225
Simultaneous rheology and cure kinetics dictate thermal post-curing of thermoset composite resins for material extrusion
공공데이터포털
Thermoset composite structures printed at room temperature using direct ink writing often collapse during thermal post-curing. This behavior suggests that the rheological properties that govern structural stability (i.e., storage modulus and/or yield stress) are sensitive to both temperature and conversion. The rheo-Raman instrument provides a way to directly link rheological properties, temperature, and conversion. Using this technique, we characterized how the yield stress and storage modulus evolve as a function of conversion at different temperatures and filler contents of fumed silica. This data set focuses on a diglycidyl ether of bisphenol A (DGEBA) epoxy resin (Epon 826, Hexion, Ohio, USA) cured with Jeffamine D-230 (Huntsman Corporation, Texas, USA). Three resins with fumed silica (Cabot Corporation, Massachusetts, USA) mass fractions of 0 %, 5 %, and 10 % were cured and observed isothermally at 70 °C and 100 °C. Rheological and Raman data were obtained, analyzed, and then combined to determine how the yield stress and storage modulus evolve with conversion at different temperatures. These results motivated a two-step schedule designed to prevent a reduction in rheological properties during curing while quickly driving the reaction to high conversion. The two-step schedule began at 70 °C then ramped to 100 °C and is also included in this dataset. This data is described in: Romberg, S.K., & Kotula, A.P. (2023) Simultaneous rheology and cure kinetics dictate thermal post-curing of thermoset composite resins, National Institute of Standards and Technology, submitted for publication.
Simultaneous rheology and cure kinetics dictate thermal post-curing of thermoset composite resins for material extrusion
공공데이터포털
Thermoset composite structures printed at room temperature using direct ink writing often collapse during thermal post-curing. This behavior suggests that the rheological properties that govern structural stability (i.e., storage modulus and/or yield stress) are sensitive to both temperature and conversion. The rheo-Raman instrument provides a way to directly link rheological properties, temperature, and conversion. Using this technique, we characterized how the yield stress and storage modulus evolve as a function of conversion at different temperatures and filler contents of fumed silica. This data set focuses on a diglycidyl ether of bisphenol A (DGEBA) epoxy resin (Epon 826, Hexion, Ohio, USA) cured with Jeffamine D-230 (Huntsman Corporation, Texas, USA). Three resins with fumed silica (Cabot Corporation, Massachusetts, USA) mass fractions of 0 %, 5 %, and 10 % were cured and observed isothermally at 70 °C and 100 °C. Rheological and Raman data were obtained, analyzed, and then combined to determine how the yield stress and storage modulus evolve with conversion at different temperatures. These results motivated a two-step schedule designed to prevent a reduction in rheological properties during curing while quickly driving the reaction to high conversion. The two-step schedule began at 70 °C then ramped to 100 °C and is also included in this dataset. This data is described in: Romberg, S.K., & Kotula, A.P. (2023) Simultaneous rheology and cure kinetics dictate thermal post-curing of thermoset composite resins, National Institute of Standards and Technology, submitted for publication.
A Materials Properties Dataset for Elastomeric Foam Impact Mitigating Materials
공공데이터포털
The database includes mechanical data for structure-properties relationships and mechanical modeling of elastic impact protection foams from a variety of imaging (micro-computed tomography, digital image correlation) and force-sensing instruments (dynamic mechanical analysis, universal test system) under a wide range of experimental conditions and modes. The data repository includes directories for: dynamic mechanical analysis raw data, results, and analysis tools; intermediate rate (servo-hydraulic UTS based) raw data including 2D digital image correlation (DIC) images, results, and analysis tools; quasi-static rate (electro-mechanical UTS based) raw data including 2D digital image correlation (DIC), results, and analysis tools; micro-computed tomography data including raw volume images, filtered images, binarized images, other results, and analysis tools; and, instrumented drop tower data including backface force, high speed video, and results and analyzed data, Fourier Transform Infrared (FTIR) spectra, and differential scanning calorimetry (DSC) data.For more information see the readme and data documentation in each respective directory. A paper describing data collection, analysis, and database documentation is available here: https://doi.org/10.1038/s41597-023-02092-4. A repository containing example usage code is available at: https://github.com/materials-data-facility/foam_db. File formats for data include .txt, .xls, .tri, .tprc, .rcp, .py, .m, .csv, .mat, .vtk, .spa, .exp, .stl, and .tif.
A Materials Properties Dataset for Elastomeric Foam Impact Mitigating Materials
공공데이터포털
The database includes mechanical data for structure-properties relationships and mechanical modeling of elastic impact protection foams from a variety of imaging (micro-computed tomography, digital image correlation) and force-sensing instruments (dynamic mechanical analysis, universal test system) under a wide range of experimental conditions and modes. The data repository includes directories for: dynamic mechanical analysis raw data, results, and analysis tools; intermediate rate (servo-hydraulic UTS based) raw data including 2D digital image correlation (DIC) images, results, and analysis tools; quasi-static rate (electro-mechanical UTS based) raw data including 2D digital image correlation (DIC), results, and analysis tools; micro-computed tomography data including raw volume images, filtered images, binarized images, other results, and analysis tools; and, instrumented drop tower data including backface force, high speed video, and results and analyzed data, Fourier Transform Infrared (FTIR) spectra, and differential scanning calorimetry (DSC) data.For more information see the readme and data documentation in each respective directory. A paper describing data collection, analysis, and database documentation is available here: https://doi.org/10.1038/s41597-023-02092-4. A repository containing example usage code is available at: https://github.com/materials-data-facility/foam_db. File formats for data include .txt, .xls, .tri, .tprc, .rcp, .py, .m, .csv, .mat, .vtk, .spa, .exp, .stl, and .tif.
In situ thermography of the metal bridge structures fabricated for the 2018 Additive Manufacturing Benchmark Test Series (AM-Bench 2018)
공공데이터포털
These measurements were performed as part of the 2018 Additive Manufacturing Benchmark Test Series (AM-Bench). This dataset and the associated experiments are part of a continuing series of controlled benchmark tests, in conjunction with a conference series, with two initial goals, 1) to allow modelers of Additive Manufacturing processes to test their simulations against rigorous, highly controlled additive manufacturing benchmark test data, and 2) to encourage additive manufacturing practitioners to develop novel mitigation strategies for challenging build scenarios. More information regarding the AMBench 2018 study can be found at www.nist.gov/ambench. For this year's challenge, numerous metal parts of the same geometry were created using an identical processing condition using a commercial powder bed fusion machine. The eight parts in total were manufactured in two builds. In situ thermal measurements of a select region on one of the parts within each build were acquired at 1800 frames per second. The part is a bridge structure geometry that has 12 legs of varying size (5 mm x 5 mm, 5 mm x 2.5 mm, and 0.5 mm x 5 mm), each leg is 5 mm tall, then uses a 45-degree overhang to transition into the bridge structure with a constant cross section. Each part is manufactured using 0.02 mm layer thickness, a programmed laser power of 195 W traveling at a scan speed of 800 mm/s, and the hatch spacing is 0.1 mm. The part is manufactured in 624 layers and the total build time nearly 9.5 hours. Details on the experiment can be found at www.nist.gov/ambench/amb2018-01-description, while related post-process measurement results can be found at www.nist.gov/ambench/benchmark-test-data.This dataset consists of thermal videos and MATLAB data structures for each layer. These are provided for each layer of the build and are grouped ten layers at a time in the provided zip files. The thermal videos provide an overview of the radiant temperature (not accounting for emissivity) measured during each layer, while the MATLAB structures contain the measurement data along with information on the camera timing, calibration, and process information. Two MATLAB functions are also provided. The first allows the measured radiant temperature to be converted into true temperature based on an assumed emissivity correction factor. The second function recreates the thermal video files. The second MATLAB function helps to provides context on how to interact with the MATLAB structures.For a detailed description of the dataset, please refer to the NIST Journal of Research publication, "Thermography of the Metal Bridge Structures Fabricated for the 2018 Additive Manufacturing Benchmark Test Series (AM-Bench 2018)." (in press)
Process Monitoring Dataset from the Additive Manufacturing Metrology Testbed (AMMT): RHF Experiment
공공데이터포털
This dataset includes the files pertaining to a 3D additive manufacturing experiment performed on the Additive Manufacturing Metrology Testbed (AMMT) by Ho Yeung on July 11, 2019. The experiment included 55 separate laser scanned 'pads' created on a bare-metal plate. Each pad corresponds to a different laser processing setting, described in the paper Yeung et al. 2020 (https://doi.org/10.1016/j.mfglet.2020.07.005). Files include the input command files, in-situ process monitoring data and metadata, and ex-situ microscope photographic images of the pad surfaces. This data is one of a set of 'AMMT Process Monitoring Datasets', as part of the Metrology for Real-Time Monitoring of Additive Manufacturing project at the National Institute of Standards and Technology (https://www.nist.gov/el/ammt-temps/datasets).