SRM 1947 Lake Michigan Fish Tissue
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SRM 1947 Lake Michigan Fish Tissue - This Standard Reference Material (SRM) is a frozen fish tissue homogenate that was prepared from fish collected from Lake Michigan, and is intended primarily for use in evaluating analytical methods for the determination of selected trace elements, methylmercury, total mercury, polychlorinated biphenyl (PCB) congeners, chlorinated pesticides, polybrominated diphenyl ether (PBDE) congeners, perfluoroalkyl acids (PFAAs), proximates, ?-hexabromocyclododecane (?-HBCD), caloric content, and fatty acids in fish tissue and similar matrices. All of the constituents for which certified, reference, and information mass fraction values are provided are naturally present in the fish tissue homogenate. A unit of SRM 1947 consists of five bottles, each containing approximately 8 g (wet basis) of frozen tissue homogenate. This data is public in the Certificate of Analysis for this material.
SRM 1945 Organics in Whale Blubber
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SRM 1945 Organics in Whale Blubber - This Standard Reference Material (SRM) is a frozen whale blubber homogenate intended for use in evaluating analytical methods for the determination of selected polychlorinated biphenyl (PCB) congeners, chlorinated pesticides, polybrominated diphenyl ether (PBDE) congeners, and toxaphene congeners. SRM 1945 has been reanalyzed, and the current Certificate of Analysis has values assigned for additional PCB congeners and pesticides, as well as values assigned for selected PBDE and toxaphene congeners. A unit of SRM 1945 consists of two screw-capped glass bottles, each containing approximately 15 g of frozen whale blubber homogenate. This data is public in the Certificate of Analysis for this material.
SRM 1958 Organic Contaminants in Fortified Human Serum (Freeze-Dried)
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SRM 1958 Organic Contaminants in Fortified Human Serum (Freeze-Dried) - This Standard Reference Material (SRM) is intended for use in evaluating analytical methods for the determination of selected polychlorinated biphenyl (PCB) congeners, chlorinated pesticides, and polybrominated diphenyl ether (PBDE) congeners in human serum and similar matrices. Reference values are provided for selected polychlorinated dibenzo-p-dioxins (PCDDs), polychlorinated dibenzofurans (PCDFs), non-ortho PCB congeners, perfluorinated compounds (PFCs), and serum lipid. Information values are provided for selected toxaphene congeners and hydroxylated compounds. A unit of SRM 1958 consists of five vials, each containing freeze-dried fortified human serum. Before use, the serum in each bottle must be reconstituted with 10.7 mL of distilled or HPLC-grade water. This data is public in the Certificate of Analysis for this material.
SRM 1957 Organic Contaminants in Non-Fortified Human Serum (Freeze-Dried)
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SRM 1957 Organic Contaminants in Non-Fortified Human Serum (Freeze-Dried) - This Standard Reference Material (SRM) is intended for use in evaluating analytical methods for the determination of selected polychlorinated biphenyl (PCB) congeners, chlorinated pesticides, and polybrominated diphenyl ether (PBDE) congeners in human serum and similar matrices. Reference values are provided for selected polychlorinated dibenzo-p-dioxins (PCDDs), polychlorinated dibenzofurans (PCDFs), perflourinated compounds (PFCs), and serum lipid. Information values are provided for selected hydroxylated compounds. All of the constituents for which values are provided in SRM 1957 are naturally present in the freeze-dried human serum. A unit of SRM 1957 consists of five 30 mL vials each containing freeze-dried non-fortified human serum. Before use, the serum in each vial must be reconstituted with 10.7 mL of distilled or HPLC-grade water. This data is public in the Certificate of Analysis for this material.
SRM 1944 New York/New Jersey Waterway Sediment
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SRM 1944 New York/New Jersey Waterway Sediment - Standard Reference Material (SRM) 1944 is a mixture of marine sediment collected near urban areas in New York and New Jersey. SRM 1944 is intended for use in evaluating analytical methods for the determination of selected polycyclic aromatic hydrocarbons (PAHs), polychlorinated biphenyl (PCB) congeners, chlorinated pesticides, and trace elements in marine sediment and similar matrices. Reference values are also provided for selected polybrominated diphenyl ether (PBDE) congeners, selected dibenzo-p-dioxin and dibenzofuran congeners, total organic carbon, total extractable material, and particle size characteristics. Information values are provided for selected polychlorinated naphthalenes (PCNs) and hexabromocyclododecanes (HBCDs). All of the constituents for which certified, reference, and information values are provided in SRM 1944 were naturally present in the sediment before processing. A unit of SRM 1944 consists of a bottle containing 50 g of radiation-sterilized, freeze-dried sediment. This data is public in the Certificate of Analysis for this material.
Mercury Concentrations in Seston, Mussels, Water, Sediments, and Preyfish from Lake Huron, 2022
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As part of the larger Great Lakes Cooperative Science and Monitoring Initiative (CSMI) , the U.S. Geological Survey Mercury Research Laboratory (MRL) completed a binational assessment partnering with the U.S. Environmental Protection Agency (US EPA), Environmental Climate Change Canada (ECCC), Michigan-DNR (MI-DNR), University of Minnesota-Duluth Natural Resources Research Institute (UM-NRRI), and the National Oceanographic and Atmospheric Association (NOAA), to assess contaminant concentrations within seston, mussels, preyfish, waters, and surface sediments within Lake Huron. All matrices were assessed for mercury and methylmercury concentrations to examine spatial trends of mercury within the lakes. Sediments were also analyzed for total mercury stable isotope composition to approximate sources of mercury contamination to the lake.
SRM 1953 Organic Contaminants in Non-Fortified Human Milk
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SRM 1953 Organic Contaminants in Non-Fortified Human Milk - This Standard Reference Material (SRM) is intended for use in evaluating analytical methods for the determination of selected polychlorinated biphenyl (PCB) congeners, chlorinated pesticides, polybrominated diphenyl ether (PBDE) congeners, and elements in human milk and similar matrices. Reference concentration values are provided for polychlorinated dibenzo-p-dioxins (PCDDs) and polychlorinated dibenzofurans (PCDFs), as well as some inorganic constituents. An information concentration value is provided for the PCB mixture Aroclor 1260. All of the constituents for which certified, reference, and information concentration values are provided in SRM 1953 are naturally present in the milk. A unit of SRM 1953 consists of five bottles of approximately 5 mL of frozen non-fortified human milk. This data is public in the Certificate of Analysis for this material.
Mercury Concentrations in Resident Lake Fish Sampled from Lake Clark National Park and Preserve in 2019 and 2020
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These data were collected as part of the Southwest Alaska Inventory and Monitoring Network (SWAN) freshwater contaminants protocol. The protocol outlines a framework for monitoring mercury (Hg) concentrations in resident lake fish within SWAN parks. The primary goal of this monitoring is to understand the spatial differences, temporal trends, and health ramifications of Hg contamination in resident lake fish. Monitoring relies on total Hg in fish axial muscle as an indicator of methyl Hg exposure. It targets four high-priority lakes which vary in size, depth, wetland cover, glacial influence, and Hg concentration. These lakes are located in two parks: Lake Clark National Park and Preserve (LACL) and Katmai National Park and Preserve (KATM). The focal species is lake trout (Salvelinus namaycush), a widespread, long lived, top predator in SWAN lakes. However, if other species are sampled as bycatch, they may be retained and analyzed if they represent species-specific data gaps in Hg concentration. Two broad types of data are generated from this protocol. The first type includes observations and measurements that are recorded while sampling and processing fish (e.g., length, weight, gender). The second type includes results of analyses performed by contract laboratories (e.g., age, total Hg). This particular dataset includes those two broad types of data for 49 fish sampled in 2019 and 2020 from 2 lakes in LACL: Lake Clark and Kijik Lake. Of those 49 fish, 40 were lake trout, 6 were burbot (Lota lota), 2 were Arctic grayling (Thymallus arcticus), and 1 was Arctic char (Salvelinus alpinus).