The USGS conducted a combined wastewater facility pre/post-closure groundwater assessment adjacent to an effluent-impacted reach of Fourmile Creek, Ankeny, Iowa, USA. This data release includes pharmaceutical concentration data for Fourmile Creek determined by enzyme-linked immunosorbent assay (ELISA) and HPLC-MS/MS during the period October 2012 to October 2014, along with associated HPLC-MS/MS analyte and method performance information.

The Ankeny, Iowa wastewater treatment facility (WWTF) was decommissioned in November 2013 providing a unique opportunity to characterize the impacts of WWTF discharge on water quality at the surface-water/groundwater interface in a shallow, unconfined alluvial aquifer. The Ankeny WWTF discharged treated effluent for nearly forty years into Fourmile Creek, located in Ankeny, Iowa. Dataset includes site information (Table 1), analytical methods (Table 2), piezometer water level elevations (Table 3), trace and major element concentrations collected from 2011 to 2013 before the WWTF shutdown (Table 4), and trace and major element concentration collected from 2013 to 2014 after the WWTF shutdown (Table 5).

Human-use pharmaceutical, pesticide, and wastewater indicator compounds were analyzed at the U.S. Geological Survey, National Water Quality Laboratory, Denver, Colorado, in wadeable streams in 4 Regional Stream Quality Assessments: Northeast (NESQA), Southeast (SESQA), Pacific Northwest (PNSQA) and California (CSQA). Multiple (with few exceptions) samplings occurred at each site, during base flow, between 2014 and 2017. Sites were located in the headwaters of perennial, wadeable streams in urban and agricultural watersheds. Site selection and methodology for each assessment can be found in Van Meter and others (2015), Sheibley and others (2015), Van Meter and others (2017), Coles and others (2016), Van Meter and others (2016), Journey and others (2015), and Van Meter and others (2014). Additional results for this study can be found in Bradley and others, 2020 and Mahler and others, 2020. See cross-reference section for full citation information.

Human-use pharmaceutical, pesticide, and wastewater indicator compounds were analyzed at the U.S. Geological Survey, National Water Quality Laboratory, Denver, Colorado, in wadeable streams in 4 Regional Stream Quality Assessments: Northeast (NESQA), Southeast (SESQA), Pacific Northwest (PNSQA) and California (CSQA). Multiple (with few exceptions) samplings occurred at each site, during base flow, between 2014 and 2017. Sites were located in the headwaters of perennial, wadeable streams in urban and agricultural watersheds. Site selection and methodology for each assessment can be found in Van Meter and others (2015), Sheibley and others (2015), Van Meter and others (2017), Coles and others (2016), Van Meter and others (2016), Journey and others (2015), and Van Meter and others (2014). Additional results for this study can be found in Bradley and others, 2020 and Mahler and others, 2020. See cross-reference section for full citation information.

The U.S. Geological Survey, in cooperation with the Minnesota Department of Health, conducted a study to determine the occurrence of unregulated contaminants in source and finished drinking waters throughout Minnesota. Minnesota relies on both groundwater and surface water sources for drinking water, which may be vulnerable to influences such as wastewater discharge and/or agricultural activities. Thus, drinking water facilities apply some form of treatment to source waters prior to distribution. Although drinking water treatment is mostly focused on satisfying regulatory requirements, it may provide secondary benefits for removal of unregulated contaminants. In 2019, 2021, and 2022, paired source and finished drinking water was collected from 100 facilities and characterized for select organic contaminants. Samples were analyzed for some combination of alkylphenols, benzotriazoles/benzothiazoles, hormones, illicit drugs, personal care products, pesticides, per- and polyfluoroalkyl substances, pharmaceuticals, plasticizers, and wastewater indicators, depending on potential influences from the watershed.

The U.S. Geological Survey, in cooperation with the Minnesota Department of Health, conducted a study to determine the occurrence of unregulated contaminants in source and finished drinking waters throughout Minnesota. Minnesota relies on both groundwater and surface water sources for drinking water, which may be vulnerable to influences such as wastewater discharge and/or agricultural activities. Thus, drinking water facilities apply some form of treatment to source waters prior to distribution. Although drinking water treatment is mostly focused on satisfying regulatory requirements, it may provide secondary benefits for removal of unregulated contaminants. In 2019, 2021, and 2022, paired source and finished drinking water was collected from 100 facilities and characterized for select organic contaminants. Samples were analyzed for some combination of alkylphenols, benzotriazoles/benzothiazoles, hormones, illicit drugs, personal care products, pesticides, per- and polyfluoroalkyl substances, pharmaceuticals, plasticizers, and wastewater indicators, depending on potential influences from the watershed.

This dataset presents the results of 475 unique organic compounds collected from 54 wadeable streams within the Southeastern, USA, collected within 10 weeks during 2014. Maximum and median exposure conditions were evaluated in relation to watershed characteristics and for potential biological effects. This dataset contains the summary statistics (maximum and median concentrations)of detected compounds, as well as a summary of quality-assurance (blanks and replicates) samples. Also included are the statistical summaries as related to analyte specific contaminant detection/concentration data and site-specific land-use matrices, spearman-rank correlations, and ToxCast evaluations.

This dataset presents the results of 475 unique organic compounds collected from 54 wadeable streams within the Southeastern, USA, collected within 10 weeks during 2014. Maximum and median exposure conditions were evaluated in relation to watershed characteristics and for potential biological effects. This dataset contains the summary statistics (maximum and median concentrations)of detected compounds, as well as a summary of quality-assurance (blanks and replicates) samples. Also included are the statistical summaries as related to analyte specific contaminant detection/concentration data and site-specific land-use matrices, spearman-rank correlations, and ToxCast evaluations.

The U.S. Geological Survey, in cooperation with the Minnesota Department of Health, conducted a study to determine the occurrence of unregulated contaminants in source and finished drinking waters throughout Minnesota. Minnesota relies on both groundwater and surface water sources for drinking water, which may be vulnerable to influences such as wastewater discharge and/or agricultural activities. Thus, drinking water facilities apply some form of treatment to source waters prior to distribution. Although drinking water treatment is mostly focused on satisfying regulatory requirements, it may provide secondary benefits for removal of unregulated contaminants. In 2019, 2021, and 2022, paired source and finished drinking water was collected from 100 facilities and characterized for select organic contaminants. Samples were analyzed for some combination of alkylphenols, benzotriazoles/benzothiazoles, hormones, illicit drugs, personal care products, pesticides, per- and polyfluoroalkyl substances, pharmaceuticals, plasticizers, and wastewater indicators, depending on potential influences from the watershed.

The U.S. Geological Survey, in cooperation with the Minnesota Department of Health, conducted a study to determine the occurrence of unregulated contaminants in source and finished drinking waters throughout Minnesota. Minnesota relies on both groundwater and surface water sources for drinking water, which may be vulnerable to influences such as wastewater discharge and/or agricultural activities. Thus, drinking water facilities apply some form of treatment to source waters prior to distribution. Although drinking water treatment is mostly focused on satisfying regulatory requirements, it may provide secondary benefits for removal of unregulated contaminants. In 2019, 2021, and 2022, paired source and finished drinking water was collected from 100 facilities and characterized for select organic contaminants. Samples were analyzed for some combination of alkylphenols, benzotriazoles/benzothiazoles, hormones, illicit drugs, personal care products, pesticides, per- and polyfluoroalkyl substances, pharmaceuticals, plasticizers, and wastewater indicators, depending on potential influences from the watershed.