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SRM 1450 Fibrous Glass Board: Retrospective Analysis
Thermal conductivity data acquired previously for the establishment of Standard Reference Material (SRM) 1450, Fibrous Glass Board, as well as subsequent renewals 1450a, 1450b, 1450c, and 1450d, are re-analyzed collectively and as individual data sets. Additional data sets for proto-1450 material lots are also included in the analysis (eleven data sets in total). The data cover the years 1958 to 2009; 52 years of activity by the National Institute of Standards and Technology (NIST) in developing and providing thermal insulation SRMs, specifically high-density molded fibrous-glass board, to the public. Collectively, the data sets cover two nominal thicknesses of 13 mm and 25 mm, bulk densities from 60 kg/m3 to 180 kg/m3, and mean temperatures from 100 K to 340 K. The prevailing generic model for the majority of data sets is the bilinear model in density and temperature. The regression equations are not intended to be, and cannot be, used to "re-certify" any of these previous SRMs. The results of this analysis, instead, aim to enhance our understanding of the original certificate equations derived by previous NIST (formerly the National Bureau of Standards) researchers as well as to improve the development and modeling of future thermal insulation SRMs.
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SRM 1450e Fibrous Glass Board
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SRM 1450e Fibrous Glass Board - This Standard Reference Material (SRM) is intended primarily for use in the measurement of the thermal conductivity or thermal resistance of insulation materials. SRM 1450e is a high-density fibrous glass board certified for bulk density and thermal conductivity. The SRM can be used in conjunction with ASTM C177 or ASTM C518. A unit of SRM 1450e consists of a square panel of fibrous glass and phenolic binder molded into a semi-rigid board. The nominal dimensions of a unit are 610 mm × 610 mm × 25 mm, and the bulk density of the material lot ranges from 110 kg/m3 to 154 kg/m3. Certified values of thermal conductivity are valid for mean temperatures from 280 K to 360 K and barometric pressures from 60 kPa to sea-level pressure (101.325 kPa).
Data from: Collaborative Guarded-Hot-Plate Tests between the Laboratoire national de métrologie et d'essais and the National Institute of Standards and Technology
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A collaborative study to compare the long-term measurement performance between guarded-hot-plate facilities at the Laboratoire national de métrologie et d'essais (LNE) in France and the National Institute of Standards and Technology (NIST) in the United States is presented. Thermal conductivity data were compiled from three international comparisons organized from 1997 to 2014. Measurements were conducted in accordance with standardized test methods (ISO 8302 or ASTM C 177) over a temperature range from 280 K to 320 K. Nine thermal insulating materials (either mineral fiber or expanded polystyrene) were examined covering broad ranges of bulk densities (13 kg/m3 to 200 kg/m3) and thicknesses (13 mm to 70 mm). A different set of specimens was utilized for each comparison. Results of this study indicate that, over a 17 year interval, the majority of test data from LNE and NIST agreed to within ±1.0%, or less, for mineral fiber materials and to within ±0.5%, or less, for expanded polystyrene. The long-term variability limit of 1% between the two laboratories is in good agreement with their current measurement uncertainties. Regression coefficients and their standard uncertainties for a straight-line model relating thermal conductivity to temperature from 280 K to 320 K were computed by material and laboratory. Graphical analysis of the data and corresponding fits exhibit consistent behavior by material type between the two laboratories. Sources of measurement variability are addressed. See also related: "Data from: Collaborative Guarded-Hot-Plate Tests between the National Institute of Standards and Technology and the National Physical Laboratory," accessible at https://doi.org/10.18434/M32106
Data from: Collaborative Guarded-Hot-Plate Tests between the Laboratoire national de métrologie et d'essais and the National Institute of Standards and Technology
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A collaborative study to compare the long-term measurement performance between guarded-hot-plate facilities at the Laboratoire national de métrologie et d'essais (LNE) in France and the National Institute of Standards and Technology (NIST) in the United States is presented. Thermal conductivity data were compiled from three international comparisons organized from 1997 to 2014. Measurements were conducted in accordance with standardized test methods (ISO 8302 or ASTM C 177) over a temperature range from 280 K to 320 K. Nine thermal insulating materials (either mineral fiber or expanded polystyrene) were examined covering broad ranges of bulk densities (13 kg/m3 to 200 kg/m3) and thicknesses (13 mm to 70 mm). A different set of specimens was utilized for each comparison. Results of this study indicate that, over a 17 year interval, the majority of test data from LNE and NIST agreed to within ±1.0%, or less, for mineral fiber materials and to within ±0.5%, or less, for expanded polystyrene. The long-term variability limit of 1% between the two laboratories is in good agreement with their current measurement uncertainties. Regression coefficients and their standard uncertainties for a straight-line model relating thermal conductivity to temperature from 280 K to 320 K were computed by material and laboratory. Graphical analysis of the data and corresponding fits exhibit consistent behavior by material type between the two laboratories. Sources of measurement variability are addressed. See also related: "Data from: Collaborative Guarded-Hot-Plate Tests between the National Institute of Standards and Technology and the National Physical Laboratory," accessible at https://doi.org/10.18434/M32106
Data from: Collaborative Guarded-Hot-Plate Tests between the National Institute of Standards and Technology and the National Physical Laboratory
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A bilateral study to compare guarded-hot-plate measurements at extended temperatures between laboratories at the National Institute of Standards and Technology (NIST) and the National Physical Laboratory (NPL) is presented. Measurements were conducted in accordance with standardized test methods (ISO 8302 or ASTM C177) over a temperature range from 20 °C to 160 °C (293 K to 433 K). Following a blind round-robin format, specimens of non-woven fibrous glass mat, approximately 22 mm thick and having a nominal bulk density of 200 kg/m3, were prepared and studied. Results of the study show that the thermal conductivity measurements agree over the temperature range of interest to within ±1.0 %, or less. See also related "Data from: Collaborative Guarded-Hot-Plate Tests between the Laboratoire national de métrologie et d'essais and the National Institute of Standards and Technology," accessible at https://doi.org/10.18434/T4XK5G
NIST Heat Transmission Properties of Insulating and Building Materials Database - SRD 81
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NIST has accumulated a valuable and comprehensive collection of thermal conductivity data from measurements performed with a 200-mm square guarded-hot-plate apparatus. The guarded-hot-plate test method is arguably the most accurate and popular method for determination of thermal transmission properties of flat, homogeneous specimens under steady state conditions. Several organizations, including ASTM and ISO, have standardized the method. Version 1.0 of the database includes data for over 2000 measurements, covering several categories of materials including concrete, fiberboard, plastics, thermal insulation, and rubber. The data cover a temperature range corresponding to most building applications; however, the majority of the measurements were conducted at 24° C (75° F). Web version 1.0
SRM 895 Stainless Steel (SAE 201)
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This Standard Reference Material (SRM) is in the form of chips sized between 0.50 and 1.18 mm sieve openings (35 and 16 mesh). It is intended for use primarily in chemical methods of analysis. Similar material for use in spectrometric methods of analysis is available as SRM 1297. This data is public in the Certificate of Analysis for this material.
SRM 895 Stainless Steel (SAE 201)
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This Standard Reference Material (SRM) is in the form of chips sized between 0.50 and 1.18 mm sieve openings (35 and 16 mesh). It is intended for use primarily in chemical methods of analysis. Similar material for use in spectrometric methods of analysis is available as SRM 1297. This data is public in the Certificate of Analysis for this material.
Expansivity of fused quartz glass measured within 6 x 10^-10 /K
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Supplemental material to the article "Expansivity of fused quartz glass measured within 6 x 10^-10 /K" by P F Egan in International Journal of Thermophysics 2024. The dataset and proceeding were first presented at the NCSLI Workshop & Symposium 2022 in Grapevine TX.Three datasets are included, corresponding to three separate runs (cycles of expansivity measurement).Run 1: cycled specimen FP_333 and FP_152 side-by-sideRun 2: FP_152 was potted with slip-fit tubes at its ends, and the run cycled specimen FP_333 and FP_152Potted side-by-sideRun 3: cycled specimen FP_333 and FP_154 side-by-sideThe Python file produces Fig. 2 from the article, and includes some literature/historical data on the thermal expansion of fused quartz glass
Utah FORGE: Well 16B(78)-32 DTS, RFS DSS Strain, and Absolute Strain Circulation Test Fiber Optic Data - August 2024
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This dataset contains processed fiber optic measurements collected during the extended cross-well circulation test at the Utah FORGE site in August 2024. The data was acquired from the 16B(78)-32 well using distributed fiber optic sensing (DFOS) technology, including distributed temperature sensing (DTS) on multimode fiber and distributed strain sensing (DSS) measurements on single-mode fiber. The dataset includes Brillouin absolute strain, Rayleigh frequency shift (RFS) DSS strain change, RFS DSS strain change rate, and temperature (DTS) data, all stored in HDF5 format. Time coordinates are provided in UTC, and depth measurements are given in measured depth relative to the rotary kelly bushing (MD RKB) in feet. The spatial sampling on the RFS DSS strain data and the Brillouin Absolute Total Strain data is 20 cm and the spatial sampling on the DTS data is 1m. The dataset is accompanied by a report from Neubrex, which provides further documentation.