Data associated with the manuscript "Glass microwave microfluidic devices for broadband characterization of diverse fluids" submitted to the Special Issue of the International Microwave Symposium (IMS) 2024 of IEEE Transactions of Microwave Theory and Techniques.
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Abstract from manuscript:We demonstrate a glass microwave microfluidic device for determining the permittivity of a wide range of liquid chemicals from 100 MHz to 10 GHz with relatively low uncertainty. Conventional microwave microfluidic devices use polymer-based microfluidic layers for fluid delivery, but these polymers swell in organic solvents and are not suitable for many applications. Our device incorporates glass microfluidic channels with platinum coplanar waveguides to provide a solvent-resistant architecture for broadband dielectric spectroscopy of fluids. We utilize broadband S-parameter measurements with a vector network analyzer on a wafer probing station and multiline thru-reflect-line calibrations to extract the distributed circuit parameters of transmission lines and solve for fluid permittivity. In this work, we demonstrate the utility of the device by measuring the broadband permittivity of four organic solvents difficult to measure otherwise: hexane, heptane, decane, and toluene.
Microwave oven interference measurements at 2.4 GHz
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The 2.4 GHz ISM band is shared by Wi-Fi, Bluetooth, Wireless HART, ISA100.11a, and several other industrial wireless systems. This band also includes microwave ovens which produce interference that disrupt communications within their vicinity, therefore, understanding and monitoring for interference from these types of radio emissions sources is crucial to ensure an optimal wireless user experience. Microwave ovens are common radio interference sources that disrupt the operation of the wireless networks in industrial environments. While avoiding these types of emissions would be an ideal solution, human practicalities often make the elimination of microwave ovens impossible. Therefore, understanding the properties of this common radio emission is necessary. A real-time spectrum analyzer (RTSA) was used to capture complex baseband recordings of radio frequency emissions of three different microwave ovens at 2.45 GHz. The measurement data herein may be used to replicate the interference in a laboratory setting and thereby allowing industrial wireless network integrators to evaluate the performance of their wireless networks operating concurrently with this type of interference.Disclaimer: Certain commercial equipment, instruments, or materials are identified in this publication in order to describe the experimental procedures and data adequately. Such identification is not intended to imply recommendation or endorsement by the National Institute of Standards and Technology, nor is it intended to imply that the materials or equipment identified are necessarily the best available for the purpose.
Interlaboratory comparison of cavity resonator measurements for complex permittivity to 170 GHz
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Figure data for "Interlaboratory comparison of cavity resonator measurements for complex permittivity to 170 GHz"ABSTRACT:Standards provide known right answers traceable to National Metrology Institutes. Today, no such complex permittivity standard exists, let alone one traceable to the International System of Units (SI). In response, a consortium of industrial, academic, and government laboratories - led by the International Electronics Manufacturing Initiative (iNEMI) - performed an interlaboratory comparison to understand the impact of this problem and how a new standard could help. The goal of the comparison was to benchmark the best-case interlaboratory agreement in complex permittivity measurements up to 170 GHz and provide some industry-led guidance for making the standard useful. The consortium used four different types of commercial resonators from 10 GHz to 170 GHz. Here, we show how we improved the best-case repeatability and interlaboratory agreement of these resonator measurements. We leverage the broader capabilities of nine industry (e.g., Intel, Panasonic, 3M) and government (e.g., NIST, ITRI) labs worldwide in the four interlaboratory comparisons presented here. These interlaboratory comparisons quantify interlaboratory agreement and incorporate stakeholder feedback to develop a fit-for-purpose standard for complex permittivity.